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中药超微粉碎技术提高愈风宁心片溶出度的研究
添加时间:2016-04-08    阅读次数:3872

1、YIQIYUSHIYAO

BJ-2XINGBENGJIEYI(TIANJINSHIGUOMINGYIYAOSHEBEIGONGSI);RCZ-8AXINGZHINENGYAOWURONGCHUYI(TIANJINDAXUEJINGMIYIQICHANG); LC-10A GAOXIAOYEXIANGSEPUYI(LC-10AD BENG,SPD-10AUV JIANCEQI,C-R7A SHUJUCHULIJI),Shim-Pack-ODS

搜狐足彩 (6.0×150mm)ZHU;JL9200 JIGUANGLIDUYI(JINANWEINAYIQIYOUXIANGONGSI);GEGENSUDUIZHAOPIN (ZHONGGUOYAOPINSHENGWUZHI

PINJIANDINGSUO);GEGENYAOCAI(GOUYUSHANXIZHENPINGXIANYIYAOGONGSI),JINGJIANDINGWEIDOUKEZHIWUYEGEPueraria lobata(Willd.)Ohwi

搜狐足彩 DEGANZAOGEN;SF-60 XINGPUTONGFENSUIJI(CHANGSHUZHONGYAOZHIYAOJIXIECHANG);SHIYANXINGWEIFENJIJIACHUN、YICHUNWEIFENXICHUN。

2、SHIYANFANGFA

2.1YANGPINZHIBEI

2.1.1GEGENJINGAOTIQU

搜狐足彩 QUGEGENCUFEN850g,YONG85% YICHUNJIAREHUILIUTIQUSANCI,DIYICIJIA8BEILIANGTIQU4XIAOSHI,DIER、SANCIGEJIA

6BEILIANGTIQU3XIAOSHI,FANGCHULVGUO,HEBINGLVYE,HUISHOUYICHUN,JIANYANONGSUOZHIXIANGDUIMIDUWEI1.32(70℃)FANGCHUJIDE。

搜狐足彩 2.1.2GEGENXIFENDEZHIBEIJILIDUFENBUJIANCHA

XIFENA:YONGPUTONGFENSUIJI(LUODI100MU)JIANGGEGENPIANFENSUIHOUZAIGUO200MUXISHAIJIDE。

XIFENB:MEICIQUGEGENPIAN400gTOUJINWEIFENJIFENSUI13FENZHONG(CISHIJIANJINGSHIYANYI100%GUO200MUSHAIQUEDING)FANGCHUJIDE。

LIDUFENBUJIANCHA:LIYONGJIGUANGLIDUYIDUIXIFENA、XIFENBDELIDU(0.6~90µm)FENBUQINGKUANGJINXINGLEJIANCE。

2.1.3PIANJIZHIBEI(SUPIAN)

PIANA:QUGEGEN(850g)TIQUJINGAOYUXIFENA 150gHUNHEGANZAO,FENSUIHOUGUO100MUSHAIJIASHILIANGDIANFEN、SUOJIAJI

搜狐足彩 XIANWEISUHUNYUN,YONG70% YICHUNRUNSHIZHILI、GANZAOZHENGLI,JIA0.5%YINGZHISUANMEIHUNYUNHOUYAPIAN1000PIAN(PIANZHONG220mg)。

PIANB:QUGEGEN(850g)TIQUJINGAOYUXIFENB 150g HUNHEGANZAO,FENSUIHOUGUO100MUSHAIJIASHILIANGDIANFEN、SUOJIAJI

XIANWEISUHUNYUN,YONG70% YICHUNRUNSHIZHILI、GANZAOZHENGLI,JIA0.5%YINGZHISUANMEIHUNYUNHOUYAPIAN1000PIAN(PIANZHONG220mg)。

搜狐足彩 2.2RONGCHUDUYANJIU

2.2.1SEPUTIAOJIAN

YONGSHIBAWANJIGUIWANJIANHEGUIJIAOWEITIANCHONGJI;LIUDONGXIANG:JIACHUN-SHUI(25∶75);LIUSU1ml·min-1;ZHUWENWEISHIWEN;

JIANCEBOZHANGWEI250nm。

2.2.2BENGJIEDUCEDING

搜狐足彩 AN《ZHONGGUOYAODIAN》2000NIANBANYIBUPIANJITONGZEXIANGXIABENGJIESHIXIANDEJIANYANFANGFA,QUSANPIPIANAYANGCEDEDEBENGJIESHIXIAN

FENBIEWEI42±3min,44±2min,45±2min;QUSANPIPIANBYANGCEDEDEBENGJIESHIXIANFENBIEWEI43±3min,45±2min,

45±7min;JUNFUHEQIGUIDING。

2.2.3XIANXINGFANWEI

JINGMICHENGQUGEGENSUDUIZHAOPIN10mg,ZHI25mlLIANGPINGZHONG,JIA30%YICHUNXISHIZHIKEDU,YAOYUN;FENBIEJINGMILIANGQU0.5,1.0,2.0,3.0,4.0,5.0ml,ZHI10ml LIANGPINGZHONG,YONG30%YICHUNXISHIZHIKEDU,ZAISHANGSHUSEPUTIAOJIANXIACEDINGGEGENSU

SEPUFENGMIANJI。YINONGDUCWEIHENGZUOBIAO,FENGMIANJIAWEIZONGZUOBIAO,ANZUIXIAOERCHENGFAJINXINGXIANXINGHUIGUI, DEHUIGUIFANGCHENGC=7.92

搜狐足彩 ×10-2A – 1.86×10-1,r=0.9992,GEGENSUHANLIANGZAI20~200µg·ml-1XIANXINGGUANXILIANGHAO。

2.2.4YANGPINZHONGGEGENSUHANLIANGCEDING

搜狐足彩 QUYUFENGNINGXINPIAN10PIAN(SUPIAN),JINGMICHENGDING,YANXI,QUXIFENYUE50mg,JINGMICHENGDING,ZHIJUSAIZHUIXINGPINGZHONG,JING

MIJIARU30%YICHUN50ml,BISAICHENGDINGZHONGLIANG,CHAOSHENGCHULI20min,CHENGDINGZHONGLIANG,YONG30%YICHUNBUZUJIANSHIDEZHONGLIANG,YAO

YUN,LVGUO,QUXULVYEZUOGONGSHIPINRONGYE;QUGONGSHIPINRONGYE10µl,JINYANGCEDING,DEPIANADEHANLIANGWEI13.62mg/PIAN(n=3),

PIANBDEHANLIANGWEI17.43mg/PIAN(n=3)。

2.2.5RONGCHUDUCEDING

ANZHAO《ZHONGGUOYAODIAN》2000NIANBANERBURONGCHUDUCEDINGFANGFAZHONGDEDIYIFACEDING,YISHUIWEISHIFANGJIEZHI,MEIZHIZHUANLANZHONG

FANGZHI3PIAN,CEDEDERONGCHULIANGWEIPINGJUNRONGCHULIANG;ZHUANSUWEI100r.min-1,PINGXINGDUIPIANA、PIANBGECE6ZU。

3、JIEGUO

搜狐足彩 3.1XIFENA、XIFENBDELIDUFENBUCESHIJIEGUO

BIAO1  XIFENADELIDUFENBUQINGKUANG

   XUHAO   LIDU(um)  TIJI%    LEIJI%    XUHAO   LIDU(um)   TIJI%    LEIJI%                                                        

1     0.6-1.2      0.000      0.00      15     27-30        2.302      14.59

搜狐足彩 2     1.2-3.0      0.000      0.00      16     30-34        2.532      17.12

3     3.0-4.5      0.006      0.01      17     34-38        3.276      20.40

搜狐足彩 4     4.5-6.2      0.372      0.38      18     38-42        3.757      24.16

5     6.2-7.6      0.534      0.91      19     42-46        4.102      28.26

6     7.6-9.2      0.802      1.71      20     46-50        4.306      32.57

7     9.2-11.4     0.871      2.58      21     50-54        4.402      36.97

搜狐足彩 8    11.4-12.8     1.089      3.67      22     54-58        4.688      41.66

9    12.8-14.2     1.102      4.77      23     58-62        10.372     52.03

搜狐足彩    10    14.2-15.8     1.123      5.89      24     62-66        14.249     66.28

   11    15.8-17       1.151     7.04       25     66-70        17.901     84.18

搜狐足彩    12    17-20        1.301     8.34       26     70-75        15.618     99.80

搜狐足彩    13    20-24        1.682     10.02      27     75-80        0.201      100.00

   14    24-27        2.266     12.29      28     80-90        0.000      100.00          

BIAO2  XIFENBDELIDUFENBUQINGKUANG

搜狐足彩   XU HAO   LIDU(um)  TIJI%    LEIJI%      XU HAO     LIDU(um)  TIJI%    LEIJI%                                                        

1     0.6-0.9      0.000     0.00         15       14-17         5.167    32.32

2     0.9-1.3      1.824     1.82         16       17-20        6.079     38.40

3     1.3-2.0      3.445     5.27         17       20-24        6.890     45.29

4     2.0-2.5      1.216     6.48         18       24-28        7.599     52.89

搜狐足彩 5     2.5-3.2      0.810     7.29         19       28-32        7.801     60.69

6     3.2-4.0      1.014     8.31         20       32-36        7.497     68.19

搜狐足彩 7     4.0-5.2      1.419     9.73         21       36-40        7.36      75.58

搜狐足彩 8     5.2-6.0      0.912     10.64        22       40-45        7.194     82.78

9     6.0-6.8      1.216     11.85        23       45-52        6.687     89.46

搜狐足彩 10    6.8-7.7      1.722     13.58        24       52-60        5.268     94.73

11    7.7-8.7      2.330     15.91        25       60-70        3.445     98.18

搜狐足彩 12    8.7-9.9      3.040     18.95        26       70-75        1.732     99.91

搜狐足彩 13    9.9-12      3.749     22.70        27       75-80        0.089     100.00

14    12-14       4.458     27.15        28       80-90       0.000      100.00                                              

ZHU:200MUSHAIKONGNEIJINGWEI75μm,300MUSHAIKONGNEIJINGWEI47μm,5μmXIANGDANGYU2000MU。

搜狐足彩 3.2RONGCHUDUCEDINGJIEGUO

搜狐足彩 BIAO3  YUFENGNINGXINPIANLEIJIRONGCHULV(%)

       SHIJIAN/min      A          B       SHIJIAN/min      A            B

搜狐足彩         10        3.2±1.6    6.5±7.2    40       42.9±1.5   71.3±1.4

        15        7.8±8.1   16.2±1.4    45       56.2±2.3    82.4±1.8

        20       11.5±5.3   26.7±2.1    50       62.1±5.6    91.6±4.1

        25       17.8±4.3   34.2±1.7    55       66.8±7.5    93.2±5.8

搜狐足彩         30       24.6±6.1   45.6±8.2    60       69.6±6.4    96.8±5.2

        35       31.4±2.6   56.4±5.2          

ZHU:n=6

搜狐足彩 3.3PIANA、PIANBRONGCHUDUBIJIAO

搜狐足彩 BIAO4  YUFENGNINGXINPIANRONGCHUDUBIJIAO

YANG  PIN                  T50/min             P

A                    43.2±6.1          <0.01

搜狐足彩                 B                    32.5±3.5

 

3.4TONGZHONGFENSUIGONGYIJISHUZHIBEIBUTONGPICIZHIJIDERONGCHUDUWENDINGXINGBIJIAO

BIAO5 YUFENGNINGXINPIANBUTONGPICIJIANRONGCHUDUBIJIAO

YANG  PIN    PI   HAO            T50/min            P

                       010426            43.5±5.6

搜狐足彩                A       010427            48.6±2.6         <0.05

                       010428            58.5±6.2

搜狐足彩                        010424            32.8±1.7

                B      010422            33.2±3.4         >0.05

010421            33.0±1.2

 

4、TAOLUN

4.1ZHIWUXIBAOZHONGDEYOUXIAOCHENGFENXUJINGGUOJINRUN、RONGZHANG、SHENTOUHEKUOSANFANGNENGRONGCHU,CHAOXIFENSUIJISHUYIFANGMIANKESHISHENG

搜狐足彩 YAOXIFENDEBIAOMIANJIDADAZENGJIA,TIGAOYAOWUDERONGCHUSUDU,CONGERYOULIYUYAOWUDEXISHOU[4];LINGYIFANGMIANCHAOXIFENSUIJISHU

KESHIZHIWUYAOXIBAOPOBILVDA90%,CONGERSHIZHIWUXIBAOZHONGDEYOUXIAOCHENGFENZHIJIEBAOLUCHULAIBINGJINRUTIYE,TIGAOQISHENGWU

搜狐足彩 LIYONGDU[5],ZHEISHIBENSHIYANZHONGCHAOXIFENSUIJISHUZHIDEDEZHIJIRONGCHUDUYUANDAYUPUTONGFENSUIJISHUZHIDEDEZHIJIDEYUANYINSUOZAI。

搜狐足彩 YOUGUANBENSHIYANZHIJIDESHENGWULIYONGDUYOUDAIJINYIBUYANJIU。

搜狐足彩 4.2GUTIZHIJIDERONGCHUDUYUYUANFULIAODEWUHUAXINGZHI、ZHIJIGONGYIDENGYINSUMIQIEXIANGGUAN,BUTONGCHANGJIAYINCAIYONGBUTONGDEYUAN

FULIAOHESHENGCHANFANGFA,BIRANZAOCHENGRONGCHUDUYOUJIAODACHAYI,JIANYIYINGTONGGUOYANJIUDUIYUFENGNINGXINPIANRONGCHUDUZUOCHUTONGYIDEPINGJIA

BIAOZHUNJIKONGZHIBIAOZHUN,YICIBAOZHENGQILINCHUANGLIAOXIAO。

搜狐足彩 4.3CAIYONGPUTONGFENSUIJISHUHUODEDEYUFENGNINGXINPIANBUTONGPICIJIANRONGCHUDUCUNZAIJIAODACHAYI,YUANYINKENENGYUQIHUODEDEYAO

搜狐足彩 FENBUNENGQUANBUWEIGUOSHAIYOUGUAN,GEGENXIANWEIXINGJIAOQIANG,LIYONGPUTONGFENSUIJIBUNENGJIAGONGZHIQUANBUWEIDADAOWEIMIZHONGYAO(1~75µm)

DEXIDU,BUJINMEICIFENSUISUODEDEXIFENZAILIDUSHANGCHAYIDA, ERQIEZAISUOHANZUZHIHUOBUWEISHANGYIYOUCHAYI,JINERSUOHANYOU

XIAOCHENGFENYEJIUBUTONG;CHAOXIFENSUIJINGGUOSHIYANQUEDINGCHUQUANGUOSHAI(200MU)FENSUISHIJIANSHIYIYAOCAIQUANBURU

搜狐足彩 YAOWEIQIANTIDE,SUOYIGEPICIZHIJIANCHAYIHENXIAO,YOUCIKANLAI, LIYONGCHAOXIFENSUIJISHUHUODEDESHENGYAOFENZHIJI,GENGFUHEZHONG

YICHUFANGYONGYAODEYAOQIU。

4.4ZHUANLANFACEDINGRONGCHUDUTONGCHANGWEIMEILANFANG1PIAN,KAOLVDAOBENSHIYANHANLIANGCEDINGFANGFADEXIANXINGFANWEIJIPIANJIDEGEGENSU

搜狐足彩 HANLIANG,GAIWEIMEILANFANG3PIAN。

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